We offer a complete material characterisation analytical service


Confidential professional service

State of the art techniques

  • some instrumentation and methods unique to Optas Ltd

5-7 day turn-around normal with rapid (24hr) turnaround available

Full written report with data interpretation

Techniques offered


FTIR Fourier Transform Infra Red Spectroscopy

provides molecular and chemical information
sample types:- solid substrates, liquids, gases, thin films
;

an extensive range of sampling accessories include

Golden Gate,

ATR (liquid and solid),

Grazing angle,

RAIRS,

Hot Stage (liquid trough)

(up to 200°C),

DRIFT

FTIR-M Fourier Transform Infra Red Microscopy

provides molecular and chemical information
FTIR microscopy applications include micro-particles (5-100mm), defects, 2D mapping of surfaces

FTIR-M-Vapour Generation Instrument

we have a brand new accessory that combines the Infra Red microscopy with a cell that controls both temperature and humidity accurately, allowing chemical changes to be monitored as a function of varying temperature and relative humidity

DSC Differential Scanning Calorimetry

measurement of thermal effects of materials
provides information about melting behaviour, glass transition temperature, crystallisation, solid-solid transitions, chemical reactions, decomposition

TGA Thermogravimetric Analysis

provides information on the content of volatile components such as solvents or water
provides information on hydration, decomposition behaviour, ash, filler content
 


DVS Dynamic Vapour Sorption Analysis

automated analysis of water sorption properties of materials
provides information on hydration, diffusion and permeability, sorption/desorption isotherms, kinetics of water uptake, activation energies and heats of sorption and desorption, moisture content. Applications include pharmaceutical powders and complexes, films, paper, food, fibres

Organic DVS

automated analysis of organic vapour sorption properties of materials
provides information on crystallinity, diffusion and permeability: sorption/desorption isotherms, kinetics of uptake, activation energies and heats of sorption and desorption, moisture content.

Organic DVS Applications

include hydrophbic pharmaceutical powders and formulations, where water sorption is poor or extremely slow, or where crystallisation is carried out from organic solvents; in these cases water sorption is not always able to measure the full extent of amorphous material

DCA Dynamic Contact Angle Analysis

contact angle and surface tension measurements; interfacial tension measurements (Du Nouy ring)
applications include wettability, surface energy, homogeneity, topography and adsorption of solids and films; wicking rate absorption, fibre perimeter and solid density measurements

DIFT Dynamic Interfacial Tension Measurements

real time interfacial tension measurements using the pendant drop method
applications include kinetic measurements of the development of the interface; measurement of the visco-elastic behaviour and interfacial rheological characteristics

Ellipsometry

refractive index properties of bulk materials, thickness and refractive index properties of thin films, sub-nanometer resolution
applications include metals, semiconductors, insulators, polymers, biomaterials

ToF-SIMS Time of Flight Secondary Ion Mass Spectrometry

ultra-sensitive surface analysis
provides molecular, ionic and chemical information of the outermost surface of substrates and films (ppm-ppb sensitivity)
applications include metals, semiconductors, insulators, polymers, biomaterials, contaminants

XPS X-ray photoelectron spectroscopy

surface analysis
provides elemental and chemical information of the outermost surface of substrates and films (0.1% sensitivity)
applications include metals, semiconductors, insulators, polymers, biomaterials, contaminants

AFM Atomic Force Microscopy (Scanning Probe Microscopy)

high resolution physical characterisation of surfaces and adsorbed materials
provides topographical informationand chemical heterogeneity of the surface properties of materials at nanometer resolution
applications include metals, semiconductors, insulators, polymers, biomaterials
 

SEM Scanning Electron Microscopy

high resolution image analysis
provides topographical information of surfaces and interfaces
applications include metals, semiconductors, insulators, polymers, biomaterials

XRD X-Ray Diffraction

x-ray diffraction analysis for comparison of physical form of pharmaceutical powders






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